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If I read correctly you have XP installed on one partition on one drive and wish to create a second partition on the same physical drive, is that correct?
If so you have approached it rather back to front, you should have created the second partition when installing XP, to do so now you risk over writing XP files if you create a new partition.
Back up all your data, then reinstall XP, creating the second partition at the appropriate time during the install phase, I prefer to just create the XP partition during this phase and format the second partition from within Windows Disk management after XP is installed.
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